269-3746 Nicolet RaptIR X Safety Information and Site Preparation Manual

Use this manual:

• Before the instrument arrives at your facility

• When preparing the installation site

• When planning electrical, environmental, and utility requirements

• When reviewing safety considerations for the instrument

This document does not include detailed instructions for operating or maintaining the instrument.

For information on installation procedures, operation, maintenance, and troubleshooting, refer to the full User Manual provided with the instrument or available through the product documentation portal (https://knowledge1.thermofisher.com).

This manual focuses on:

• Site preparation and facility requirements

• High-level safety information and hazard awareness

• Responsibilities for safe installation and integration

The Nicolet™ RaptIR™ X may present the following types of hazards:

Even when the instrument is used as intended, some risks may remain.

Examples include:

• Exposure to hazardous materials introduced by the user.

• Environmental conditions that affect safe operation.

• Improper integration into a larger system.

These risks can be minimized by following the safety guidance in this manual and the User Manual.

To reduce risk:

• Follow all safety instructions and warnings in the documentation.

• Ensure the installation environment meets specified requirements.

• Use appropriate personal protective equipment (PPE).

• Only use approved accessories and compatible materials.

• Ensure all personnel are properly trained.

When it is equipped with the Nicolet™ RaptIR™ X SAM, the system is a Class 1 laser system according to IEC 60825-1.

The laser classification indicates the level of hazard associated with accessible laser radiation. Class 1 lasers are eye-safe and are safe during normal use.

To reduce the risk of injury:

• Never look directly into the laser beam

• Do not expose eyes or skin to laser radiation

• Follow all warning labels and safety instructions

• Use the instrument only as described in the documentation

• Operate the instrument only with all protective housings and covers in place

• Do not modify the laser or optical components

• Ensure that only trained personnel operate the instrument

Improper use of the laser may result in hazardous radiation exposure.

The instrument includes laser safety labels that provide important hazard information.

The Nicolet™ RaptIR™ X microscope was designed for the following environmental conditions. Ensure that the installation site meets these requirements to ensure optimal performance and to avoid damage to the instrument.

Provide sufficient space for:

• Installation and system access.

• Cable connections and routing.

• Ventilation and heat dissipation.

• Service and maintenance access.

Allow clearance around the instrument to ensure proper airflow and accessibility. Additional space is recommended to improve usability and serviceability.

The installation surface must:

• Support the total system weight, including accessories.

• Support placement of computer peripherals, such as keyboard and mouse.

• Be stable and level.

• Minimize vibration.

Vibration or instability may affect system performance and measurement quality.

Floor vibration or acoustical noise from heavy manufacturing equipment or other sources will not damage the system, but it can affect performance and spectral quality.

Keep the system away from machinery that may vibrate the floor, and minimize or eliminate acoustic noise and vibration wherever possible.

Ensure adequate ventilation around the instrument.

Do not block ventilation openings or restrict airflow.

Avoid placing the instrument near:

• Heating or cooling vents

• Heat-generating equipment

• Direct sunlight

Proper airflow is necessary to maintain stable operating conditions.

Install the instrument in a well-lit environment that allows safe operation and maintenance.

Avoid conditions that may interfere with visibility or safe handling of samples.

The following table lists the specifications for electrical service. Contact our service representative in your area if you have questions about the requirements.

If you are not sure that your power lines meet these requirements, contact technical support for information about power audits.

Power supplied to the system must be stable and free of excessive fluctuations, interruptions, or electrical noise.

Generally, 50% more power should be available than the entire system (including accessories) typically uses. Maximum power consumption and heat dissipation specifications for the microscope and accessories are shown below. The values are approximate.

Values shown are estimates. Refer to the power specifications on the rear panels or undersides of these units.

Each wall outlet you use must be equipped with a 3-wire line: live, neutral, and ground. The ground must be a non-current-carrying wire connected to earth ground at the main distribution box.

To enure a good ground connection and avoid shock hazard, do not use an outlet that has ground connected to a conduit ground.

Ensure that the power disconnect device (such as a plug or circuit breaker):

• Is easily accessible to the operator.

• Can be quickly disconnected in an emergency.

• Is located near the instrument.

Be sure to use an appropriate power cord for the electrical service.

The power cord supplied with the accessories is a 3-wire grounded power cord appropriate for use in the country listed as the shipping destination for the microscope.

To prevent electrical hazards, do not remove or defeat the ground prong on the power cord.

If you use an extension cord, it must have a protective ground conductor.

If the power cord becomes damaged, replace it. Contact us if you need additional information about replacement cords or extension cord specifications.

Depending on the system configuration, the Nicolet™ RaptIR™ X microscope may require one or more of the following utilities:

• Gas supply (for example, dry air or nitrogen)

• Ventilation or exhaust

• Cooling (if applicable)

• Network or communication connections

• DVD drive connected to the computer — OMNIC™ Paradigm™ software and any other software purchased with your system comes on a DVD. If you are installing the software from the disc, your computer will need a DVD drive.

Refer to product-specific specifications for exact requirements.

The Nicolet™ RaptIR™ X weights a maximum of 70.3 kb (155 lbs) and has the following dimensions:

• Microscope dimensions:

  • Wide: 49.2 cm

  • Deep: 74.3 cm

  • Tall: 64.1 cm

• Microscope with SAM dimensions

  • Wide: 78.9 cm

  • Deep: 78.2 cm

  • Tall: 64.1 cm

Use only accessories and components approved by the manufacturer.

Some accessories require specific utilities, connections, or environmental conditions. Ensure all requirements are met before installation.

Use of unapproved accessories may result in equipment damage or unsafe operation.

Some configurations require a supply of clean, dry gas for purging or operation.

If a purge gas supply is required:

• Use only clean, dry air or nitrogen. Both dry air and nitrogen effectively remove water vapor and solvents from the system. If you want to remove carbon dioxide from the system as well, use a source of dry air with a carbon dioxide scrubber or use nitrogen as your purge gas.

• The purge gas must be free of moisture, oil, and other reactive materials. To remove particulate matter and oil, you may need to install a 10-micrometer oil-trap filter.

• The dry air or nitrogen purge gas should be dried to a dew point of -70 °C (-94 °F) or below for best performance.

If you purchased the optional purge gas fittings with your system, install the purge lines and necessary fittings before the instrument arrives.

For instructions, refer to "Purging the microscope."

Provide adequate ventilation for the installation area.

Ventilation may be required to:

• Remove heat generated by the instrument.

• Prevent accumulation of hazardous vapors from samples or solvents.

• Maintain safe working conditions.

If hazardous or volatile materials are used, additional local exhaust ventilation (such as a fume hood) may be required.

If your microscope uses a liquid nitrogen-cooled detector, you must provide a supply of liquid nitrogen and a safe method for handling and venting boil-off gases.

All utilities must:

• Be accessible for operation and service

• Be controllable by the user or facility

• Comply with applicable local codes and regulations

It is important that all utilities are installed and accessible before system installation.

When the instrument arrives:

• Inspect the shipping container for visible damage

• Do not accept or open damaged shipments without guidance from the manufacturer

• Report any damage immediately

If the shipping container appears damaged, contact us for instructions.

Your microscope will be unpacked and installed by one of our service representatives, and that person will check for damage and will verify that the shipment is complete.

• Keep the shipping container upright at all times

• Use appropriate equipment (such as pallet jacks or carts) when moving the shipment

• Avoid sudden impacts, tilting, or dropping the container

Move the shipping box to the installation location at least 24 hours before installation to allow the system to acclimate. Allowing the system to acclimate helps prevent condensation and potential damage.

In addition to the purge kit, you will need the following:

• 3/4-inch (20 mm) open-ended wrench

• 11/16-inch (18 mm) open-ended wrench

• #2 Phillips screwdriver

• Thread seal tape ("Teflon™ tape" or "PTFE tape")

1. Connect the quick-release pressure fitting to the source of the purge gas.

   1. Install the regulator valve and either a 1/4-inch male fitting or a 3/8-inch female fitting on the purge gas source. (Choose a valve and fittings that are appropriate for the purge gas source.)

      

      Figure 1. Valve

   2. If you used a 1/4-inch male fitting, proceed to the next step.

      If you used a 3/8-inch female fitting on the purge gas source, install the 3/8-inch to 1/4-inch reducing nipple that was included with your purge kit. Wrap the reducing nipple with thread seal tape before you install it, and use an 11/16-inch open-ended wrench to tighten the connection.

      

      Figure 2. Reducer

   3. Wrap the reducing nipple or the 1/4-inch male fitting with thread seal tape, then install the pressure coupling. Use a 3/4-inch open-ended wrench to tighten the connection.

      

      Figure 3. Valve assembly

   A	3/8" to 1/4" male reducing nipple (if required)
   B	Pressure coupling
   C	Shutoff valve

2. Snap the male inlet of the wall plumbing assembly firmly into the quick-release fitting.

   

   Figure 4. Connections

   A	To microscope
   B	To spectrometer
   C	Flowmeter
   D	Pressure regulator
   E	Quick-release fitting
   F	Wall plumbing assembly

3. Connect the gas lines to the instruments.

   1. Snap the quick connect from the purge pneumatic assembly (labeled “to spectrometer”) into the purge inlet on the spectrometer’s lower rear panel.

   2. Snap the second quick connect from the purge pneumatic assembly (labeled “to microscope”) to the purge inlet on the microscope’s lower rear panel.

4. Set the purge gas controls.

   1. Rotate the main shutoff valve to the open position.

   2. On the 'to spectrometer' connection side of the assembly, pull up on the pressure regulator and set the dial to 20 PSI.

   3. Press the regulator back down.

   4. Rotate the flowmeter control to set the flow to 20 SCFH.

   5. Repeat for the second side of the purge pneumatic assembly so that the controls for both the spectrometer and the microscope are set as follows:

1. Plug in the power cord to the instruments and turn on the power.

2. Wait 30 to 60 minutes for the instrument to fully purge before you use the instrument. Continue to purge continuously. If you turn off the instrument and the purge, turn on the purge and wait 30 to 60 minutes again to fully purge the instrument before use.

The purge filter is green when dry and turns yellow when it is damp. If the filter turns yellow permanently or is otherwise discolored or contaminated with debris or oil, replace the entire purge pneumatic assembly. Contact technical support for details.